Hi Brian, We e-beam Fe quite frequently and often have problems with the users venting too soon afterwards, resulting in fractured graphite crucibles. However, I think you don't have to be too concerned with oxide if you "soak" the material before beginning the deposition. That is, run the EBEAM supply up to about 75% of your deposition power and let it sit for about 1-2min with the shutter closed. That should remove the oxide. -Mike Martin >>> gabriel.matus@gmail.com 06/10/05 12:13 PM >>> The standard pickling solution in the non MEMS world is 1 M HCl. I can't imagine your oxide is too thick so a few seconds should do the trick.