Hello, You could try to evaporate maximum 2 nm of gold over your structures in rotational mode. Fixed mode (for lift off) may work as well if you don't want to tilt your specimen. Less than2 nm of gold should be transparent to electron beam and shouldn't form crstals. Make sure you have a good contact between your sample and the SEM stage in order to dissipate the charges. Good luck Tell us what did you get Cristian On 8/16/05, Woo-Jin Changwrote: > Hi, > > I can't remember the exact name of the material, but I took SEM pictures of > PDMS, successfully, after painting the surface of PDMS. It was silver based > painting material. The supporting engineer painted the surface of PDMS with > brush, and then dried up for one day. Around 20 micron x 25 micron of > columnar structures were clearly shown. > > Sorry for insufficient information, but I think it was normally used > solution. I think you can get some information from manufacturer of SEM.