Eric, If you apply the diamond tip's along the substrate'(such as Si) crystal orientation, the cracking line can be pretty trim and the side of the substrate would be very smooth. Kind of tricky, and you may not expect 100 percent success in this way. Another way is CPM, higher possibility of success but more complicated. Good luck, Hongjun ------------------------------------ Hongjun Zeng, PhD MEMS/Nano Scientist Nanotechnology Core Facility (NCF formerly MAL) University of Illinois at Chicago -----Original Message----- From: Eric J. Correa Sent: Monday, November 07, 2005 11:36 AM To: mems-talk@memsnet.org Subject: [mems-talk] SEM Thickness Measurement Hi Everyone: I am trying to measure UNCD (diamond) thickness using a SEM by looking at the cross sectional area. I am using a diamond tip to cut my samples but I am not able to get a clean cross-sectional area. I was just wondering if anyone has any advice or recommendation.