Try the following; 1. More stable solution: 3 HCl:1 HNO3:1 H2O 2. About 2um thick positive photoresist AZ 1512 Good luck. jjiahwrote: Dear All, I am currently trying to process Broad Area Lasers on 1cm2 AlGaAs sample. On the Epi side i am depositing Ti/Au by e-beam evaporation. Then using photolithography to create openings on the sample to isolate the devices from each other by etching all the way to the substrate using wet etching. The photoresist i am using is a positive photoresist (S1813). My problem is this: I know that (3 HCl:1 HNO3) will etch Au and AlGaAs and HF will etch Ti, but my photoresist will not hold against either etchants. As a result, my photoresist will not cover and protect the areas i don't want to be etched. Can someone please suggest a solution for my problem?