Try Phosphoric acid @ 155C used for etching of LPCVD, i.e. silicon rich SiN film in Semiconductor/MEMS industry. For process details, open the Stanford Nano Fabrication (SNF) Process link as follows; http://www-snf.stanford.edu/Equipment/wbgeneral/NitrideEtchWBGen.html Ciro Chiappiniwrote: I have to etch a 2000A thick silicon rich nitride film under a photoresist (AZ5209) mask. I need to get a nitride mask since the next step is electrochemical etching in EToH:HF 3:7. I am currently RIE etching it, but the process is very time consuming. I tried wet etch both HF:H2O 1:10 AND HF:HCL 1:1 but the resist gets peeled off in few minutes. Do you have any alternative recipe to suggest?