Jay Does it look like there is Cr left on what should be bare Si after delamination? That might be important. Also, how are you measuring thickness of the deposition? What kind of boat or crucible are you using for the metals in the hot filament system and how healthy are they? As you can see, I still have more questions than answers. Typically, an O2 plasma won't adversely oxidize silicon but it won't make up for inadequate development during lithography. If the plasma process isn't tuned properly or there are problems with the resist then it can transfer material from the resist to the open areas and not provide any substantial gains in cleaning. Lower power might be better if you're worried about this. It's not conclusive but the gold underneath the peeled films suggests it's not your litho process. If everything were fine with your metal layers and a resist residue were causing delamination then you'd expect Cr coloured underside. I'd guess off the top of my head that your Au layer is being overheated during deposition, perhaps due to too high a deposition rate or the source being too close to the target. The Au might be mixing with the underlying Cr, reducing it's usefulness as an adhesion layer and giving you some Au colouration on the underside. This is mere speculation not being able to see the films. I'd have thought that the temperature required for this would adversely affect the resist or make it difficult to remove though. Anyhow, I'd try a slower deposition for Au and it couldn't hurt as someone else pointed out to put down a thicker Cr adhesion layer. Good luck, Rick