Variations are caused by variations in atmospheric humidity. Vacuum vapor prime. Vacuum dehydrates totally. HMDS vapor reacts with Hydroxyl ions on wafer and creates an inorganic molecule/organic molecule bridge. Perfect resist adhesion always. Bill Moffat ________________________________ From: mems-talk-bounces@memsnet.org on behalf of madhav rao Sent: Fri 8/15/2008 10:39 AM To: mems-talk@memsnet.org Subject: [mems-talk] Photolithography - Resist peeling Hi, I am experiencing a problem in patterning on silicon-di-oxide = wafers; I am using SHIPLEY 1818 resist to get a thickness of 2.5 micron; = 6 seconds of exposure time. After developing for 60 seconds, I observe, = the resist layer peels off; leaving no patterns on the wafer. Also I had = soft-baked the resist at 95 C for 2 minutes in hot-plate. This seems strange to me, as a month ago, I had successfully transferred = the patterns on to silicon-di-oxide wafers. I am using mylar film masks. Please let me know, if any one had experienced similar problems before; = and if so, could you let me know suggestions to solve ? Thanks Regards, Madhav Rao, Graduate student, University of Alabama.