Gary, Thanks for your response. I am going mostly by memory here. I noticed the adhesion problem by observing a difference in color between different shapes. Then when I measured with the profilometer one of them was 3.5 um and the other 160 nm thick, so at this point it was very obvious that there is a delamination problem. Further SEM measurements cleary indicated the delamination problem on the substrate. I am not sure about this but I believe the Ti layer is the only thing that stayed on the substrate and every other layer (Ag/Ti/Au) got peeled off after the lift-off. However, I don't see how oxidation can be the problem as I do not break vacuum during my depositions. Any other suggestions? Thanks again, Evelyn On Fri, Jan 16, 2009 at 11:00 AM, Gary Hillmanwrote: > Evelyn, it would seem to me that the Ti seed layer might be oxidized and > therefore the upper metal layers aren't sticking. Is the surface > discolored > by Ti and the metal above lifting off. Gary > -- EVELYN BENABE Graduate Research Assistant RF Microsystems Research Group University of South Florida 4202 East Fowler Avenue Tampa, FL 33620 Office: ENB 412 Office Phone: (813)-974-4851 Email: benabe@mail.usf.edu