Al has a good point - stylus profilometers are perfectly capable of measuring step heights around 100nm. Before you sputter, mask a small sacrificial area of your wafer with a tiny piece of Kapton tape, sputter, peel the tape off afterwards and measure the step height. Just make sure your tape is vacuum-compatible to avoid contaminating your chamber/film. Brian C. Stahl Graduate Student Researcher UCSB Materials Research Laboratory brian.stahl@gmail.com / bstahl@mrl.ucsb.edu Cell: (805) 748-5839 Office: MRL 3117A On Fri, Feb 13, 2009 at 9:13 AM, Albert Henningwrote: > Neither ellipsometry nor reflectometry will be able to measure > thicknesses of metal films in excess of about 50 nm. Thicknesses beyond > 50 nm cannot be distinguished optically from a bulk metal. OTOH, even > an ancient AlphaStep can work just fine. > > Al