Hello Evelyn, I just happen to know what happened. Oxygen plasma oxidizes platinum. You're likely measuring Pt-Ox. You can reduce the oxygen in a hydrogen atmosphere. There are a number of references in a paper I recently wrote (shameless plug): Hydrogen Detection by Polyaniline Nanofibers on Gold and Platinum Electrodes Jesse D. Fowler, Shabnam Virji, Richard B. Kaner, Bruce H. Weiller The Journal of Physical Chemistry C 2009 113 (16), 6444-6449 Jesse Fowler >From Evelyn BTo General MEMS discussion Subject [mems-talk] Ashing effects To all, I measured the average thickness of a Ti/Pt stack-up on a Si wafer at three different locations as summarized below: * Before ashing After ashing Delta* Structure #1: 139.7 nm 219.00 nm 79.30 nm Structure #2: 122.5 nm 199.75 nm 77.25 nm Structure #3: 117.0 nm 200.00 nm 83.00 nm After doing the ashing I did not observe any damage to the Pt layer but can't explain the increase in thickness above, especially when I had already calculated an etch rate of 11 nm/min and had only etched for 3 minutes. The ashing recipe is 150 W, 44 sccm, 250 mT for 3 minutes in O2 plasma (PE mode). Can anyone think of anything that could cause a change of 80 nm in thickness? -- EVELYN BENABE