Hi, I have been working with LiNbO3 and HMDS. Two things we found important: The LiNbO3 surface has to be as water-free as possible, which meant that we dried the LiNbO3 despite its pyroelectrical properties under elevated temperatures. Try to keep the temperature ramp low (2-4 deg C/min), this should prevent too much charge built-up. Secondly, a short gentle soft-bake of the resist. Best regards Holger -- Dr. Holger Becker microfluidic ChipShop GmbH Carl-Zeiss-Promenade 10 D-07745 Jena Germany Tel. .+49 (0) 36 41 347 05 80 Fax: +49 (0) 36 41 347 05 90 Geschäftsführerin: Dr. Claudia Gärtner Sitz der Gesellschaft: D-07745 Jena, Germany Amtsgericht Jena: HRB 209251 USt.-IdNr.: DE 221812444 -----Ursprüngliche Nachricht----- Von: mems-talk-bounces@memsnet.org [mailto:mems-talk-bounces@memsnet.org] Im Auftrag von Andrew Sarangan Gesendet: Freitag, 14. August 2009 05:39 An: General MEMS discussion Betreff: [mems-talk] Adhesion promoter for LiNbO3? I am having adhesion problems of photoresist on LiNbO3 substrate. I've tried HMDS (vapor prime) but it is not clear to me if HMDS works on LiNbO3. Furthermore, my problem is exacerbated by the fact that I am not doing any soft-bake or PEB, in order to avoid charge build-up on the substrate. Instead I've been drying the resist films in a vacuum at room temperature. This is Shipley 955 resist. Any thoughts would be appreciated. Thanks.