All, The holes are anywhere from 1 to 5 microns in size that I am unable to etch through. I have tried sodium lauryl sulfate as a surfactant in the Iodine etching solution with no success (even when using ultrasonic agitation). What I need (in my opinion) is a chemical etchant that's smaller than iodine & less toxic than cyanide. I need to be able to get a gold etchant through copper micro-holes (about 2 microns in size). Thanks for all your efforts, Dave Lewis Lake Shore Cryotronics Ohio Dave.Lewis@Lakeshore.com