I agree with Mike. Try using a RIE or DRIE oxygen plasma, its easy and safe. In a March 1701 RIE we would run 300-400mT of O2 at 300-400W. Though I would add that you might want to try a CF4 ~16-20% + O2 step for say 30 seconds for a little more aggressive removal of material in addition to the oxygen etch. >>> Mike Whitson6/24/2010 11:17 AM >>> The asher will eventually do the job, but you may have to let it run for a very long time, and there's a good chance you will have to contend with problems related to heating of your sample. If you have access to it, oxygen RIE can be much faster and more effective than a barrel asher. I've used a bench-top ICP- RIE to strip cross-linked PMMA with good success. If you want to be extra thorough, you can use piranha much more safely after the RIE has taken out most of the organic material - piranha can be very violent if you give it a lot of organic matter to oxidize at once. Even if you don't have a specific oxygen RIE, many DRIE tools have an oxygen cycle for chamber descumming which can also be used for organic stripping if your facility's SOP allows. Solvent-based strippers (acetone, NMP, etc.) won't help you on cross-linked resists, don't bother with those. -Mike