I am trying to fabricate ridge waveguide on X-cut LiNbO3 parallel to crystallographic Y-axis. Initially after depositing Cr-layer of specific thickness I am doing Proton Exchange in Benzoic acid to activate the unmasked surface, then I am doing RIE of the activated surface using CHF3 and Ar. But after doing RIE for ~ 10 min some white particles are observed to be grown on the surface, it has been found that the particles is Nb2O5. I don't have any clue how it is forming during etching and I want to avoid the formation of this particle. Can anybody suggest something? Thanks a lot in advance. Shantanu Pal PhD Research Scholar Integrated Optoelectronics/MEMS & Microelectronics Labs, Electrical Engineering Department, Indian Institute of Technology Madras, Chennai-600036,India.