durusmail: mems-talk: Thick AZ photoresist summary -
Thick AZ photoresist summary -
1999-05-25
Thick AZ photoresist summary -
Marc A. Unger
1999-05-25
Hi All -

About two weeks ago I inquired:

> Anyone happen to know a set of conditions for patterning an
> AZ type resist at 10-20 microns thick?

I got many responses, condensed below for anyone interested in
the summarized answers.  Thanks very much to everyone who
replied!

Marc Unger
Caltech Applied Physics,
ungerm@cco.caltech.edu

*****************

Shipley does make a thick resist. Its the SJR 5700 series. I use SJR
5740, which is is the 15 to 20 um thick version. I like this resist
alot. It works well.

   The processing is very similar to normal resist, except that after
spinning the resist must 'rest' on the chuck for 6 minutes before
softbake (the resist needs to relax). BTW the resist immediately after
spinning will look horrible, don't worry, let it rest. The softbake is
on a hot plate (not a vacuum hot plate) for 6 minutes and the
development takes 6 to 7 minutes (in shipley 354). The resulting pattern
has nice vertical sidewalls and sticks well to metal films (I haven't
used it on oxide or SiN)
[Ken Westra, ken@amc.ab.ca]

******************

AZ 4620 spun at 2k rpm will give you about 9.5-10 um
[Thomas Rocco Tsao]

******************

AZ 4620 at 3000 rpm is ~9 u.   Try 1500 rpm or so.
[Jason Tauscher
Silicon Designs, Inc.
Jason@SiliconDesigns.com
(425)391-8329]

******************

One way to achieve this is to use a thick resist - something like AZ4620
(I thinks Shipley also makes a thick resist?).
This type of photoresist can be spun on with different thicknesses (up to
100um thick) by varying the rpm spin speed and time.
[Angela Rasmussen
The George Washington University
The Institute of MEMS and VLSI Technologies

******************

AZ4903 can be spun on at 4500 rpm and baked for 90s at 115C.  This will
supply you with a 10 um film.  For resist layers thinner than 16 um, simply
slow the spin speed.  Another positive resist that can be used for thinner
films is Shipply 1045.  You should be able to get this information easily
from the resist manufacturers.
[John Williams
MEMS Network Engineer
Cornell Nanofabrication Facility
M103 Knight Laboratory
Cornell University
Ithaca, NY 14850
Ph.   (607) 255-2329 x 129
Fax  (607) 255-8601
williams@cnf.cornell.edu]

******************

Using Hoechst's AZ4562, we get 12 micron patterns with the following
conditions:

-80" spinning at 1000 rpm
-30' softbake at 100C
-90" illumination at 5 mW/cm2
-developing using AZ531 developer
-hardbake

[Dirk De Bruyker
 K.U.Leuven, Dept. Esat-Micas
Kard. Mercierlaan 94, B-3001 Leuven, Belgium
Tel: +32 16 32 1700      Fax: +32 16 32 1975
E-mail:   Dirk.DeBruyker@esat.kuleuven.ac.be
http://www.esat.kuleuven.ac.be/~debruyke]

******************

I have exposed AZ4903 resist with an i-line 10:1 reduction stepper.  At
4500 rpm, the resists spins out to ~12 microns.  Prebake done at 115 C
for 1.5 min.  Holdtime for 45 minutes to dissipate air bubbles in resist
to avoid focus problems.  Exposure time in stepper ~11 secs per die which
is quite long.   It is probably better to break up the exposures and
focus the stepper and different levels in the resist to get better
quality features but my features were quite large, 15 to 100 microns.
Developer needed is AZ 421K.
[Mark,  mez2@cornell.edu]

******************

Try a photoresist called SU-8. It can be patterned to >100 microns high with
great resolution.  Try electronic visions in Arizona to find out more about
the resist.
[BobHendu@aol.com]

******************


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