Hi Michael, Thank you very much for your informative reply. Indeed, I find there's noticeable aluminum redeposistion-like phenomenon happend after CF4 RIE etching. The trenches got contaminated and became very rough after etching. As you mentioned, I did get a few better results from the RIE equipment with ICP. However, the surface was very rough with certain particles sitting around trench edges. Still, the trench patterns were not transfer to silicon as well as expected, size shrinking and not straight edges. Actually, I tried photoresist (PMMA) rather than aluminum as mask. But I found the selectivity is not as good to protect PMMA, though the selectivity heavily depends on the recipe. Thanks, Li