Sounds like you did not expose the material properly. Gary -----Original Message----- From: mems-talk-bounces+garyh=s-cubed.com@memsnet.org [mailto:mems-talk-bounces+garyh=s-cubed.com@memsnet.org]On Behalf Of Yingtao Tian Sent: Tuesday, January 10, 2012 1:27 PM To: General MEMS discussion Subject: [mems-talk] SU-8 process development Hi Everyone, I would like to ask advice for SU-8 processing because this is my first time to use this famous stuff. I just tried to put down 4-5 um thick SU-8 5 resist and follow the recipe from MicroChem. However, I did not get anything useful. The sample was Au coated silicon wafer, soaked in acetone for 5 mins, rinsed with IPA and dried. The wafers were put in the oven at 150 degree for 20 mins to dehydrate. Spin coating consists of two steps: 500 rpm, 100 r/s acc for 10 seconds; then 4000 rpm, 500 r/s for 30 seconds. Soft bake was done at 65 C for 1 min then 95 C for 3 mins. Exposure time ranged from 7 seconds to 10 seconds. Post exposure bake was done at 65 C for 1 min and 95 C for 1 min. Development was done in EC Solvent for 10 mins. Most of the features were about 4 micron big with relatively large pitch size. However, I could not get the features cleared. Anybody has some ideas or suggestions on this? Any reply will be appreciated. Thanks, Yingtao