Mehmet, It sounds like you may be using undiluted HMDS which can react with your photoresist and render it undevelopable. We usually dilute our HMDS with Xylene (80:20 Xylene: HMDS) before the dispense/spin cycle. A 3000 rpm, 60 second spin cycle with the diluted HMDS should leave a layer that will improve adhesion without affecting the photoresist that is subsequently spin-coated. Best, Brian Baker Utah Nanofab _______________________________________________ Hosted by the MEMS and Nanotechnology Exchange, the country's leading provider of MEMS and Nanotechnology design and fabrication services. Visit us at http://www.mems-exchange.org Want to advertise to this community? See http://www.memsnet.org To unsubscribe: http://mail.mems-exchange.org/mailman/listinfo/mems-talk