We have problems regarding reactive ion etching with freon (CF_4) of thick (1-5um) SiO_2 layers. We use an old PLASMA THERM PD 2480 Plasma Etch System 1984. Problem: Even after very long etching times we observe high aspect ratio "needles" and residues at the substrate (diamond) surface. Our process parameters are: 400W, 45mTorr, 45 SCCM CF_4 We use an Al mask for etching. Thanks in advance Mario