Is the nitride has experienced a thermal oxidation process? If so, there will be a thin oxide in the surface. This thin oxide should be etched prior to the nitride etching. Additionally, 1 hour H3PO4 etching is not enough to remove 2 micron Si3N4. 2009-10-31 xudehui0108 发件人: Nor Hafizah Ngajikin 发送时间: 2009-10-30 14:35:53 收件人: mems-talk 抄送: 主题: [mems-talk] wet etch of 2um Si3N4 Dear all, I've tried to etch 2 micron thickness of Si3N4 using hot H3PO4. The concentration of H3PO4 is 85w%. I heat the H3PO4 at 150 degree celcius for 1 hour. Unfortunately, this experiment didn't work as expected. None of the nitride is etch away. Can anybody share with me your experience on nitride etch using H3PO4. Thank you. Hafizah