PMMA is notch sensitive, in addition to freezing try scribing the reverse surface of your PMMA substrate (presuming you're not already). -----Original Message----- From: mems-talk-bounces@memsnet.org [mailto:mems-talk-bounces@memsnet.org] On Behalf Of Hunter, Luke L I've found that freezing the sample in LN2 before cleaving helps. It's still not perfect and PMMA doesn't like to break cleanly but it breaks more than tears when I do this. -----Original Message----- From: mems-talk-bounces@memsnet.org [mailto:mems-talk-bounces@memsnet.org] On Behalf Of Jeff Kettle I have been patterning structures into PMMA using an Electron beam lithography system. I was wondering if anyone had any advice on capturing an image of the cross section for the patterned structure (post-development) using an SEM.